C₂₁H₃₀O₂

Base Information

Chemical Name:C₂₁H₃₀O₂
CAS No.:1334480-42-0
Molecular Formula:C₂₁H₃₀O₂
Molecular Weight:314.468
Hs Code.:

C<sub>21</sub>H<sub>30</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₀O₂

Chemical Property:

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Technology Process of C₂₁H₃₀O₂

There total 3 articles about C₂₁H₃₀O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334480-41-9,340016-57-1
C₁₉H₃₈OSn

: 1048344-88-2
C₁₅H₁₉F₃O₄S

: 1334480-42-0
C₂₁H₃₀O₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; lithium chloride; In dimethyl sulfoxide; at 60 ℃; for 24h; Inert atmosphere; Darkness;
DOI:10.1002/chem.201100425

Reference yield:

: 1048344-89-3
(2R,5R)-2,5-diallyl-2,5-dimethylcyclohexane-1,4-dione

: 1334480-42-0
C₂₁H₃₀O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 6 h / -78 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; lithium chloride / dimethyl sulfoxide / 24 h / 60 °C / Inert atmosphere; Darkness

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium hexamethylsilazane; copper(l) chloride; lithium chloride; In tetrahydrofuran; dimethyl sulfoxide; 2.1: Stille coupling;
DOI:10.1002/chem.201100425

Reference yield:

: C₁₆H₂₀O₆

: 1334480-42-0
C₂₁H₃₀O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis(3,5,3′,5′-dimethoxydibenzylideneacetone)palladium(0); (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / diethyl ether / 10 h / 25 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 6 h / -78 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; lithium chloride / dimethyl sulfoxide / 24 h / 60 °C / Inert atmosphere; Darkness

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(3,5,3′,5′-dimethoxydibenzylideneacetone)palladium(0); potassium hexamethylsilazane; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; copper(l) chloride; lithium chloride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; 3.1: Stille coupling;
DOI:10.1002/chem.201100425