C₂₈H₂₄Cl₃N₃OS

Base Information

Chemical Name:C₂₈H₂₄Cl₃N₃OS
CAS No.:1394867-52-7
Molecular Formula:C₂₈H₂₄Cl₃N₃OS
Molecular Weight:556.943
Hs Code.:

C<sub>28</sub>H<sub>24</sub>Cl<sub>3</sub>N<sub>3</sub>OS

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Chemical Property of C₂₈H₂₄Cl₃N₃OS

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Technology Process of C₂₈H₂₄Cl₃N₃OS

There total 4 articles about C₂₈H₂₄Cl₃N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1394867-89-0
2-{3-(4-chlorobenzoyl)-4-[(4-(3,4-dichlorophenyl)piperazin-1-yl)methyl]-5-phenylthiophen-2-yl}isoindoline-1,3-dione

: 1394867-52-7
C₂₈H₂₄Cl₃N₃OS

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Inert atmosphere; Reflux;
DOI:10.1021/jm3007504

Reference yield:

: 1027493-29-3
2-[5-bromo-3-(4-chloro-benzoyl)-4-methyl-thiophen-2-yl]-isoindole-1,3-dione

: 1394867-52-7
C₂₈H₂₄Cl₃N₃OS

Guidance literature:: Multi-step reaction with 4 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; cesium fluoride; water / 1,4-dioxane / 5.5 h / Inert atmosphere; Heating

2: N-Bromosuccinimide; dibenzoyl peroxide / 1,2-dichloro-ethane / 3 h / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere; Cooling with ice

4: hydrazine hydrate / ethanol / 1 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; hydrazine hydrate; triethylamine; cesium fluoride; dibenzoyl peroxide; In 1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm3007504

Reference yield:

: 98-80-6
phenylboronic acid

: 1394867-52-7
C₂₈H₂₄Cl₃N₃OS

Guidance literature:: Multi-step reaction with 4 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; cesium fluoride; water / 1,4-dioxane / 5.5 h / Inert atmosphere; Heating

2: N-Bromosuccinimide; dibenzoyl peroxide / 1,2-dichloro-ethane / 3 h / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere; Cooling with ice

4: hydrazine hydrate / ethanol / 1 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; hydrazine hydrate; triethylamine; cesium fluoride; dibenzoyl peroxide; In 1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm3007504