Technology Process of C11H16N2O
There total 4 articles about C11H16N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
In
ethanol;
at 20 ℃;
for 72h;
under 15001.5 Torr;
DOI:10.1021/ic3020749
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Novozyme 435 / 4 h / 20 °C
2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
2.2: 1 h / 0 °C
3.1: trimethylsilylazide; tetrabutyl ammonium fluoride / neat (no solvent) / 96 h / 85 °C / Cooling with ice
4.1: hydrogen / ethanol / 72 h / 20 °C / 15001.5 Torr
With
trimethylsilylazide; tetrabutyl ammonium fluoride; hydrogen; sodium hydride;
In
tetrahydrofuran; ethanol;
DOI:10.1021/ic3020749
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylsilylazide; tetrabutyl ammonium fluoride / neat (no solvent) / 96 h / 85 °C / Cooling with ice
2: hydrogen / ethanol / 72 h / 20 °C / 15001.5 Torr
With
trimethylsilylazide; tetrabutyl ammonium fluoride; hydrogen;
In
ethanol;
DOI:10.1021/ic3020749