Technology Process of C22H29IN2O3
There total 1 articles about C22H29IN2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetraethylammonium fluoride / acetonitrile / 16 h / 40 °C / Inert atmosphere
2.1: 4-methyl-morpholine; benzotriazol-1-ol / dichloromethane / 0 °C / Inert atmosphere
2.2: 16 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; tetraethylammonium fluoride; benzotriazol-1-ol;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201100180
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; Tetrabutylammoniumsalz der Diphenylphosphinsaeure;
In
N,N-dimethyl-formamide;
for 0.166667h;
Inert atmosphere;
DOI:10.1002/chem.201100180
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere
2.1: 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure;
In
dichloromethane; N,N-dimethyl-formamide;
1.1: Stille coupling;
DOI:10.1002/chem.201100180
