C₃₈H₃₈N₄O₁₂

Base Information

Chemical Name:C₃₈H₃₈N₄O₁₂
CAS No.:1320252-27-4
Molecular Formula:C₃₈H₃₈N₄O₁₂
Molecular Weight:742.739
Hs Code.:

C<sub>38</sub>H<sub>38</sub>N<sub>4</sub>O<sub>12</sub>

Synonyms:

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Chemical Property of C₃₈H₃₈N₄O₁₂

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Technology Process of C₃₈H₃₈N₄O₁₂

There total 9 articles about C₃₈H₃₈N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1320252-14-9
(+)-(2S,3aS,8aS)-trimethyl 3a-amino-3,3a-dihydropyrrolo[2,3-b]indole-1,2,8(2H,8aH)-tricarboxylate

: 1320252-27-4
C₃₈H₃₈N₄O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: chlorosulfonic acid; triethylamine / dichloromethane / 1.08 h / 0 - 23 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / Inert atmosphere

3.1: dmap / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

3.2: 12 h / 23 °C / Inert atmosphere

4.1: BEMP on polystyrene resin / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

4.2: 0.25 h / 23 °C / Inert atmosphere

5.1: tert-butyl alcohol / 5 h / 23 °C / UV-irradiation; Inert atmosphere

With chlorosulfonic acid; dmap; oxalyl dichloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja2057852

Reference yield:

: 1320252-13-8
(+)-(2S,3aS,8aS)-trimethyl 3a-azido-3,3a-dihydropyrrolo[2,3-b]indole-1,2,8(2H,8aH)-tricarboxylate

: 1320252-27-4
C₃₈H₃₈N₄O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: DL-dithiothreitol; triethylamine / methanol / 0.33 h / 23 °C / Inert atmosphere

2.1: chlorosulfonic acid; triethylamine / dichloromethane / 1.08 h / 0 - 23 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / Inert atmosphere

4.1: dmap / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

4.2: 12 h / 23 °C / Inert atmosphere

5.1: BEMP on polystyrene resin / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

5.2: 0.25 h / 23 °C / Inert atmosphere

6.1: tert-butyl alcohol / 5 h / 23 °C / UV-irradiation; Inert atmosphere

With chlorosulfonic acid; dmap; oxalyl dichloride; DL-dithiothreitol; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja2057852

Reference yield:

: 1320252-24-1
C₃₈H₄₀N₆O₁₄S

: 1320252-27-4
C₃₈H₃₈N₄O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: BEMP on polystyrene resin / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

1.2: 0.25 h / 23 °C / Inert atmosphere

2.1: tert-butyl alcohol / 5 h / 23 °C / UV-irradiation; Inert atmosphere

With BEMP on polystyrene resin; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1021/ja2057852