10-chloropulegone

Base Information

• Chemical Name: 10-chloropulegone
• CAS No.: 94994-47-5
• Molecular Formula: C₁₀H₁₅ClO
• Molecular Weight: 186.681
• Mol file: 94994-47-5.mol

Synonyms:

Chemical Property of 10-chloropulegone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 10-chloropulegone

There total 2 articles about 10-chloropulegone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-chloro-isopulegol (74514-24-2) → 10-chloropulegone (94994-47-5,94994-48-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 3.18 g / CrO₃, H₂O, concd. H₂SO₄ / acetone

2: 0.84 g / triethylamine / 8 h / Heating

With chromium(VI) oxide; sulfuric acid; water; triethylamine; In acetone;

DOI:10.1021/jo00206a039

Reference yield:

10-chloroisopulegone (94994-46-4) → 10-chloropulegone (94994-47-5,94994-48-6) + (+)-menthofuran (17957-94-7)

Guidance literature:

With triethylamine; for 8h; Heating;

DOI:10.1021/jo00206a039

upstream raw materials:

10-chloroisopulegone

10-chloro-isopulegol