trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline

Base Information

Chemical Name:trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline
CAS No.:103620-26-4
Molecular Formula:C₁₃H₁₁NO₂
Molecular Weight:213.236
Hs Code.:

trans-7,8-dihydroxy-7,8-dihydrobenzo<f>quinoline

Synonyms:

Suppliers and Price of trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline

Chemical Property:

Purity/Quality:

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Technology Process of trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline

There total 2 articles about trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.5%

: 103639-19-6
trans-7,8-diacetoxy-7,8-dihydrobenzoquinoline

: 103620-26-4,114416-29-4,87707-06-0
trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline

Guidance literature:: With sodium hydroxide; In methanol; for 0.25h;
DOI:10.1021/jo00368a001

Reference yield:

: 103620-25-3,103667-11-4
Acetic acid (7S,8S)-8-acetoxy-10-bromo-7,8,9,10-tetrahydro-benzo[f]quinolin-7-yl ester

: 103620-26-4,114416-29-4,87707-06-0
trans-7,8-dihydroxy-7,8-dihydrobenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / tetrahydrofuran / 12 h / 0 - 5 °C

2: 29.5 percent / 2percent NaOH / methanol / 0.25 h

With sodium hydroxide; DBN; In tetrahydrofuran; methanol;
DOI:10.1021/jo00368a001