N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester

Base Information

• Chemical Name: N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester
• CAS No.: 213773-54-7
• Molecular Formula: C₁₆H₁₈F₄N₂O₄S₂
• Molecular Weight: 442.456

Synonyms:

Chemical Property of N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester

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Technology Process of N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester

There total 1 articles about N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

2,5-dithia cyclohexanone (74637-14-2) + N-glycyl-4-amino-N-butyric acid 2,3,5,6-tetrafluorophenyl ester trifluoroacetate → N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester (213773-54-7)

Guidance literature:

In chloroform; water; for 8h; Ambient temperature; phosphate buffer, pH 6;

DOI:10.1039/a804717k

Reference yield: 70.0%

ORe(3+) (110943-22-1,12060-05-8,12624-27-0) + N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester (213773-54-7) → ReO(C16H17F4N2O4S2)2(1+)*Cl(1-)*CH3COOC2H5 = [ReO(C16H17F4N2O4S2)2]Cl*CH3COOC2H5

Guidance literature:

In water; isopropyl alcohol; (argon); addn. of aq. oxorhenium(V) gluconate to th ligand in i-PrOH, stirring (room temp., 5 min); addn. of H2O and EtOAc, layer sepn., washing (brine), drying (MgSO4), evapn. , treatment with Et2O; elem. anal.;

DOI:10.1039/a804717k

Reference yield: 22.0%

tetra-n-butylammonium tetrachlorooxorhenate(V) + N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyric acid 2,3,5,6-tetrafluorophenyl ester (213773-54-7) → [2,3,5,6-tetrafluorophenyl N-(N-5-sulfanyl-3-thiapentanoyl)glycyl-4-aminobutyrate(3-)]oxorhenium(V)

Guidance literature:

With NaOAc; In methanol; (argon); addn. of the Re complex salt in MeOH to the ligand and NaOAc inMeOH at 0°C, stirring (room temp., 28 h); solvent removal (vac.); chromy. (SiO2; EtOAc/i-PrOH), evapn., dissoln. (MeCN), chromy. (MeCN/H2O, at last MeCN), evapn. (vac.); elem. anal.;

DOI:10.1039/a804717k

upstream raw materials:

2,5-dithia cyclohexanone

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