((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

Base Information

Chemical Name:((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))
CAS No.:445263-21-8
Molecular Formula:C₅₁H₄₇IrOP₂Si
Molecular Weight:958.187
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3P)2Ir(CO)(CHCHCHC(C<sub>6</sub>H<sub>5</sub>)C(Si(CH<sub>3</sub>)3))

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Chemical Property of ((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

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Technology Process of ((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

There total 2 articles about ((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 445263-18-3
(Z)-3-(2-iodoethenyl)-1-phenyl-2-(trimethylsilyl)-1-cyclopropene

: 445263-22-9
[Ir(CO)(PPh3)(η5-C5H3Ph(SiMe3))]

: 445263-20-7
((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

: 445263-21-8
((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

Guidance literature:: With n-butyl lithium; In diethyl ether; hexane; n-BuLi/hexane slowly added to soln. of cyclopropene in Et2O at -78°C, stirred at -78°C for 15 min, mixt. slowly added to suspn. ofIr compd. in Et2O at -78°C, mixt. stirred at -78°C for 0. 5 h, slowly warmed to room temp.; evapd. (vac.), residue chromd. (silica gel, hexane/Et2O (8/1)), mixt. ofcomplexes obtained (yield 47%), Iridabenzvalene isolated by treating th e mixt. with MeI (excess) for 0.5 and successive filtration; elem. anal.;
DOI:10.1021/om700336d

Reference yield:

: 59246-46-7,14871-41-1,15318-31-7
bis(triphenylphosphine)carbonyliridium(I) chloride

: C₆H₅CC(Si(CH₃)3)CHCHCHI

: 445263-22-9
[Ir(CO)(PPh3)(η5-C5H3Ph(SiMe3))]

: 445263-20-7
((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

: 445263-21-8
((C₆H₅)3P)2Ir(CO)(CHCHCHC(C₆H₅)C(Si(CH₃)3))

Guidance literature:: With BuLi; In diethyl ether; BuLi was added at -78°C to soln. iodide in Et2O, (PPh3)2Ir(CO)Cl was added at -78°C and allowed to warm to room temp. for 3 h;
DOI:10.1021/om0201563