C₆₅H₉₆N₄O₄

Base Information

• Chemical Name: C₆₅H₉₆N₄O₄
• CAS No.: 1414964-73-0
• Molecular Formula: C₆₅H₉₆N₄O₄
• Molecular Weight: 997.502
• Mol file: 1414964-73-0.mol

Synonyms:

Chemical Property of C₆₅H₉₆N₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₅H₉₆N₄O₄

There total 4 articles about C₆₅H₉₆N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pentaerythritol (115-77-5) → C65H96N4O4 (1414964-73-0)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine / Inert atmosphere; Schlenk technique

2: sodium azide / Inert atmosphere; Schlenk technique

3: palladium on activated charcoal; hydrogen / Inert atmosphere; Schlenk technique

4: ethanol / 12 h / Reflux; Schlenk technique; Inert atmosphere

With pyridine; sodium azide; palladium on activated charcoal; hydrogen; In ethanol;

DOI:10.1039/c4ra02092h

Reference yield:

1,3-diazido-2,2-bis(azidomethyl)propane (31107-13-8) → C65H96N4O4 (1414964-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / Inert atmosphere; Schlenk technique

2: ethanol / 12 h / Reflux; Schlenk technique; Inert atmosphere

With palladium on activated charcoal; hydrogen; In ethanol;

DOI:10.1039/c4ra02092h

Reference yield:

2,2-bis(((methylsulfonyl)oxy)methyl)propane-1,3-diyl dimethanesulfonate (7511-62-8) → C65H96N4O4 (1414964-73-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide / Inert atmosphere; Schlenk technique

2: palladium on activated charcoal; hydrogen / Inert atmosphere; Schlenk technique

3: ethanol / 12 h / Reflux; Schlenk technique; Inert atmosphere

With sodium azide; palladium on activated charcoal; hydrogen; In ethanol;

DOI:10.1039/c4ra02092h

upstream raw materials:

tetrakis(aminomethyl)methane

3,5-di-tert-butyl-2-hydroxybenzaldehyde

Pentaerythritol

2,2-bis(((methylsulfonyl)oxy)methyl)propane-1,3-diyl dimethanesulfonate

Refernces