C₁₃H₁₉N₂O₆P

Base Information

Chemical Name:C₁₃H₁₉N₂O₆P
CAS No.:289492-03-1
Molecular Formula:C₁₃H₁₉N₂O₆P
Molecular Weight:330.277
Hs Code.:

C<sub>13</sub>H<sub>19</sub>N<sub>2</sub>O<sub>6</sub>P

Synonyms:

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Chemical Property of C₁₃H₁₉N₂O₆P

Chemical Property:

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Technology Process of C₁₃H₁₉N₂O₆P

There total 6 articles about C₁₃H₁₉N₂O₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 289492-01-9
C₁₅H₂₃N₂O₆P

: 289492-03-1
C₁₃H₁₉N₂O₆P

Guidance literature:: With lithium hydroxide; triethylamine carbonate; In methanol; acetonitrile; at 20 ℃; for 14h;
DOI:10.1016/S0960-894X(00)00186-4

Reference yield:

: 621-84-1
O-benzyl carbamate

: 289492-03-1
C₁₃H₁₉N₂O₆P

Guidance literature:: Multi-step reaction with 6 steps

1: 60 percent / AcOH / 3 h / 20 - 85 °C

2: 72 percent / MeONa; NaOH / 2 h / 20 °C

3: 86 percent / NaOH; aq. HCl / methanol / 12 h / 20 °C

4: SOCl₂ / CH₂Cl₂ / 4 h / 20 °C

5: 46 percent / Et₃N / CHCl₃ / 240 h / 20 °C

6: LiOH; triethylammonium bicarbonate / acetonitrile; methanol / 14 h / 20 °C

With hydrogenchloride; lithium hydroxide; sodium hydroxide; thionyl chloride; sodium methylate; triethylamine carbonate; acetic acid; triethylamine; In methanol; dichloromethane; chloroform; acetonitrile; 1: Condensation / 2: transesterification / 3: Hydrolysis / 4: Chlorination / 5: Substitution / 6: Hydrolysis;
DOI:10.1016/S0960-894X(00)00186-4

Reference yield:

: 61989-17-1
N-benzyloxycarbonyl-1-aminoethanephosphonic acid methyl monoester

: 289492-03-1
C₁₃H₁₉N₂O₆P

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / CH₂Cl₂ / 4 h / 20 °C

2: 46 percent / Et₃N / CHCl₃ / 240 h / 20 °C

3: LiOH; triethylammonium bicarbonate / acetonitrile; methanol / 14 h / 20 °C

With lithium hydroxide; thionyl chloride; triethylamine carbonate; triethylamine; In methanol; dichloromethane; chloroform; acetonitrile; 1: Chlorination / 2: Substitution / 3: Hydrolysis;
DOI:10.1016/S0960-894X(00)00186-4