C₃₁H₃₁⁽²⁾H₃N₂O₃Si

Base Information

Chemical Name:C₃₁H₃₁⁽²⁾H₃N₂O₃Si
CAS No.:1352941-12-8
Molecular Formula:C₃₁H₃₄N₂O₃Si
Molecular Weight:513.684
Hs Code.:

C<sub>31</sub>H<sub>31</sub><sup>(2)</sup>H<sub>3</sub>N<sub>2</sub>O<sub>3</sub>Si

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Chemical Property of C₃₁H₃₁⁽²⁾H₃N₂O₃Si

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Technology Process of C₃₁H₃₁⁽²⁾H₃N₂O₃Si

There total 12 articles about C₃₁H₃₁⁽²⁾H₃N₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352941-05-9
C₃₂H₃₄N₂O₄Si

: 1352941-12-8
C₃₁H₃₁⁽²⁾H₃N₂O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.25 h / -78 °C / Inert atmosphere

1.3: -78 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.83 h / 0 °C / Inert atmosphere

2.2: 1.5 h / 0 - 20 °C / Air atmosphere

2.3: 1.33 h / -78 - 20 °C / Inert atmosphere

3.1: TBAF on alumina / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: caesium carbonate / 144 h / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; TBAF on alumina; caesium carbonate; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jo202286a

Reference yield:

: 1352941-10-6
C₄₆H₄₃N₃O₆Si

: 1352941-12-8
C₃₁H₃₁⁽²⁾H₃N₂O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: TBAF on alumina / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2: caesium carbonate / 144 h / Inert atmosphere

With TBAF on alumina; caesium carbonate; In tetrahydrofuran;
DOI:10.1021/jo202286a

Reference yield:

: 1352941-06-0
C₃₆H₃₉N₃O₄Si

: 1352941-12-8
C₃₁H₃₁⁽²⁾H₃N₂O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.83 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 0 - 20 °C / Air atmosphere

1.3: 1.33 h / -78 - 20 °C / Inert atmosphere

2.1: TBAF on alumina / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

3.1: caesium carbonate / 144 h / Inert atmosphere

With lithium aluminium tetrahydride; TBAF on alumina; caesium carbonate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo202286a