dichloro(2,6-lutidine)phenylgold(III)

Base Information

Chemical Name:dichloro(2,6-lutidine)phenylgold(III)
CAS No.:380650-18-0
Molecular Formula:C₁₃H₁₄AuCl₂N
Molecular Weight:452.133
Hs Code.:

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Chemical Property of dichloro(2,6-lutidine)phenylgold(III)

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Technology Process of dichloro(2,6-lutidine)phenylgold(III)

There total 2 articles about dichloro(2,6-lutidine)phenylgold(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: gold(III) chloride

: 768-32-1
trimethylphenylsilane

: 15439-85-7
2,6-lutidine hydrochloride

: 380650-18-0
dichloro(2,6-lutidine)phenylgold(III)

Guidance literature:: gold(III) chloride; trimethylphenylsilane; In hexane; at -78 - 20 ℃; for 0.5h;

2,6-lutidine hydrochloride; In diethyl ether; hexane; for 1h; Reagent/catalyst;
DOI:10.1021/ja408712e

Reference yield: 30.0%

: 108-48-5
2,6-dimethylpyridine

: 21563-00-8
gold(III) chloride

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 380650-18-0
dichloro(2,6-lutidine)phenylgold(III)

Guidance literature:: In diethyl ether; hexane; byproducts: HCl; under N2; benzene added to hexane suspn. of Au complex (molar ratio 40:1) at 20°C; stirred for 30 min; Et2O added; filtered; filtrate treated with Et2O soln. of 2,6-lutidine (2 equiv.); stirred at room temp. for 1 h; volatiles removed in vac.; chromd. (silica gel, benzene-hexane); pale yellow fraction collected; recrystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1039/b102527a

Reference yield:

: 1003-09-4
2-bromothiophene

: 380650-18-0
dichloro(2,6-lutidine)phenylgold(III)

: 29488-24-2
2-Bromo-5-phenyl-thiophene

Guidance literature:: With silver trifluoromethanesulfonate; In chloroform-d1; 1,2-dichloro-ethane; at 20 ℃; for 0.333333h; Darkness;
DOI:10.1021/ja408712e