Technology Process of C35H31NS4
There total 8 articles about C35H31NS4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: thionyl chloride / dichloromethane / 2 h / 20 °C
2: aluminum (III) chloride / dichloromethane / 20 °C
3: tin(ll) chloride; hydrogenchloride / ethanol; water / 80 °C
4: toluene-4-sulfonic acid / toluene / 110 °C / Dean-Stark
5: titanium trichloride tris(tetrahydrofuran); zinc / tetrahydrofuran / 1 h / 40 °C / Inert atmosphere
6: dichloromethane / UV-irradiation
With
hydrogenchloride; aluminum (III) chloride; thionyl chloride; titanium trichloride tris(tetrahydrofuran); toluene-4-sulfonic acid; tin(ll) chloride; zinc;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
2: |Friedel-Crafts Acylation / 4: |Paal-Knorr Pyrrole Synthesis / 5: |McMurry Reaction;
DOI:10.1016/j.tet.2014.06.005
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aluminum (III) chloride / dichloromethane / 20 °C
2: tin(ll) chloride; hydrogenchloride / ethanol; water / 80 °C
3: toluene-4-sulfonic acid / toluene / 110 °C / Dean-Stark
4: titanium trichloride tris(tetrahydrofuran); zinc / tetrahydrofuran / 1 h / 40 °C / Inert atmosphere
5: dichloromethane / UV-irradiation
With
hydrogenchloride; aluminum (III) chloride; titanium trichloride tris(tetrahydrofuran); toluene-4-sulfonic acid; tin(ll) chloride; zinc;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
1: |Friedel-Crafts Acylation / 3: |Paal-Knorr Pyrrole Synthesis / 4: |McMurry Reaction;
DOI:10.1016/j.tet.2014.06.005
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tin(ll) chloride; hydrogenchloride / ethanol; water / 80 °C
2: toluene-4-sulfonic acid / toluene / 110 °C / Dean-Stark
3: titanium trichloride tris(tetrahydrofuran); zinc / tetrahydrofuran / 1 h / 40 °C / Inert atmosphere
4: dichloromethane / UV-irradiation
With
hydrogenchloride; titanium trichloride tris(tetrahydrofuran); toluene-4-sulfonic acid; tin(ll) chloride; zinc;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
2: |Paal-Knorr Pyrrole Synthesis / 3: |McMurry Reaction;
DOI:10.1016/j.tet.2014.06.005