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cis-Pt(PMe2Ph)2(SiPh3)CH2CD3

Base Information
  • Chemical Name:cis-Pt(PMe2Ph)2(SiPh3)CH2CD3
  • CAS No.:273217-80-4
  • Molecular Formula:C36H42P2PtSi
  • Molecular Weight:762.819
  • Hs Code.:
cis-Pt(PMe<sub>2</sub>Ph)2(SiPh<sub>3</sub>)CH<sub>2</sub>CD<sub>3</sub>

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Chemical Property of cis-Pt(PMe2Ph)2(SiPh3)CH2CD3
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Technology Process of cis-Pt(PMe2Ph)2(SiPh3)CH2CD3

There total 1 articles about cis-Pt(PMe2Ph)2(SiPh3)CH2CD3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; pentane; under N2, pentane soln. of Li-compd. and Pt-complex were mixed, THF wasadded at 0 °C, mixt. was stirred at room temp. for 30 min; MeOH was slowly added, mixt. was evapd. to dryness by pumping, solid was extd. 3 times with CH2Cl2, soln. was filtered through Celite, soln. was concd., Et2O was layered, layer was allowed to stand at -70 °C overnight;
DOI:10.1021/om000012t
Guidance literature:
In benzene-d6; under N2, 10-fold excess of Ph2C2, heating at 40 °C; monitored by (2)D NMR;
DOI:10.1021/om000012t
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