[2-methoxy-4-[7-methoxy-6-(4-methylphenyl)sulfonyloxy-1-oxo-3a,4,9,9a-tetrahydro-3H-benzo[f][2]benzofuran-4-yl]phenyl] 4-methylbenzenesulfonate

Base Information

• Chemical Name: [2-methoxy-4-[7-methoxy-6-(4-methylphenyl)sulfonyloxy-1-oxo-3a,4,9,9a-tetrahydro-3H-benzo[f][2]benzofuran-4-yl]phenyl] 4-methylbenzenesulfonate
• CAS No.: 17768-66-0
• Molecular Formula: C₃₄H₃₂O₁₀S₂
• Molecular Weight: 664.754
• NSC Number: 32997,32996
• DSSTox Substance ID: DTXSID60938976
• Mol file: 17768-66-0.mol

Synonyms:17768-66-0;NSC32996;6323-26-8;DTXSID60938976;NSC32997;NSC-32996;NSC-32997;2-Methoxy-4-{7-methoxy-6-[(4-methylbenzene-1-sulfonyl)oxy]-1-oxo-1,3,3a,4,9,9a-hexahydronaphtho[2,3-c]furan-4-yl}phenyl 4-methylbenzene-1-sulfonate

Chemical Property of [2-methoxy-4-[7-methoxy-6-(4-methylphenyl)sulfonyloxy-1-oxo-3a,4,9,9a-tetrahydro-3H-benzo[f][2]benzofuran-4-yl]phenyl] 4-methylbenzenesulfonate

Chemical Property:

• Vapor Pressure: 8.33E-29mmHg at 25°C
• XLogP3: 6.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 9
• Exact Mass: 664.14368956
• Heavy Atom Count: 46
• Complexity: 1260

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)OC2=C(C=C(C=C2)C3C4COC(=O)C4CC5=CC(=C(C=C35)OS(=O)(=O)C6=CC=C(C=C6)C)OC)OC

Technology Process of [2-methoxy-4-[7-methoxy-6-(4-methylphenyl)sulfonyloxy-1-oxo-3a,4,9,9a-tetrahydro-3H-benzo[f][2]benzofuran-4-yl]phenyl] 4-methylbenzenesulfonate

There total 2 articles about [2-methoxy-4-[7-methoxy-6-(4-methylphenyl)sulfonyloxy-1-oxo-3a,4,9,9a-tetrahydro-3H-benzo[f][2]benzofuran-4-yl]phenyl] 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + 3a,4,9,9a-tetrahydro-6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-7-methoxynaphtho[2,3-c]furan-1(3H)-one (5474-93-1) → bis-O-(toluene-4-sulfonyl)-β-conidendrin (6323-26-8,17768-66-0)

Guidance literature:

With pyridine;

DOI:10.1021/ja01152a131

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → bis-O-(toluene-4-sulfonyl)-α-conidendrin (6323-26-8,17768-66-0)

Guidance literature:

With pyridine;

DOI:10.1021/jo01179a009

upstream raw materials:

p-toluenesulfonyl chloride

3a,4,9,9a-tetrahydro-6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-7-methoxynaphtho[2,3-c]furan-1(3H)-one