4-Nitrobenzo[cd]indol-2(1h)-one

Base Information

Chemical Name:4-Nitrobenzo[cd]indol-2(1h)-one
CAS No.:28440-62-2
Molecular Formula:C₁₁H₆N₂O₃
Molecular Weight:214.18
Hs Code.:
NSC Number:116386
DSSTox Substance ID:DTXSID50297504
Wikidata:Q82038624

Synonyms:28440-62-2;4-nitrobenzo[cd]indol-2(1h)-one;NSC116386;DTXSID50297504;NSC-116386

Suppliers and Price of 4-Nitrobenzo[cd]indol-2(1h)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-Nitrobenzo[cd]indol-2(1h)-one

Chemical Property:

Vapor Pressure:0.000236mmHg at 25°C
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:214.03784206
Heavy Atom Count:16
Complexity:339

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC2=CC(=CC3=C2C(=C1)NC3=O)[N+](=O)[O-]

Technology Process of 4-Nitrobenzo[cd]indol-2(1h)-one

There total 4 articles about 4-Nitrobenzo[cd]indol-2(1h)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-nitro-1,3-dioxo-1H-benzo [de]isoquinolin-2(3H)-yl p-toluensulfonate

: 28440-61-1
7-nitrobenzo[cd]indol-2(1H)-one

: 28440-62-2
3-Nitro-naphthostyril

Guidance literature:: With sodium hydroxide; In ethanol; water; for 1h; Overall yield = 97percent; Overall yield = 390 mg; Reflux;
DOI:10.1016/j.ejmech.2019.05.086

Reference yield:

: 301337-46-2
8-bromo-3-nitro-[1]naphthoic acid

: 28440-62-2
3-Nitro-naphthostyril

Guidance literature:: With ammonia; water; at 150 ℃; unter Druck;

Reference yield:

: 3027-38-1
3-nitro-1,8-naphthalic anhydride

: 28440-61-1
7-nitrobenzo[cd]indol-2(1H)-one

: 28440-62-2
3-Nitro-naphthostyril

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; hydroxylamine hydrochloride / 1 h / Reflux

1.2: 2 h / Reflux

2.1: sodium hydroxide / water; ethanol / 1 h / Reflux

With pyridine; hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water;
DOI:10.1016/j.ejmech.2019.05.086