1,2,4-OXADIAZOLE-3-CARBONYLCHLORIDE

Base Information

• Chemical Name: 1,2,4-OXADIAZOLE-3-CARBONYLCHLORIDE
• CAS No.: 39512-69-1
• Molecular Formula: C₃HClN₂O₂
• Molecular Weight: 132.506
• Mol file: 39512-69-1.mol

Synonyms:

Chemical Property of 1,2,4-OXADIAZOLE-3-CARBONYLCHLORIDE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1,2,4-Oxadiazole-3-carbonyl chloride 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,4-OXADIAZOLE-3-CARBONYLCHLORIDE

There total 2 articles about 1,2,4-OXADIAZOLE-3-CARBONYLCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1,2,4]oxadiazole-3-carboxylic acid hydrazide (39512-60-2) → [1,2,4]oxadiazole-3-carbonyl chloride (39512-69-1)

Guidance literature:

With hydrogenchloride; chlorine; In methanol; nitromethane;

DOI:10.1039/P19730000047

Reference yield:

→ [1,2,4]oxadiazole-3-carbonyl chloride (39512-69-1)

Guidance literature:

3-CO-NH-NH2-Verb., HCl;

Reference yield:

(4-chlorobenzyl)triphenylphosphonium bromide (51044-12-3) + [1,2,4]oxadiazole-3-carbonyl chloride (39512-69-1) → 2-(4-chloro-phenyl)-1-[1,2,4]oxadiazol-3-yl-2-(triphenyl-λ5-phosphanylidene)-ethanone (51791-17-4)

Guidance literature:

Multistep reaction; (i) NaOEt, EtOH, (ii) /BRN= 508444/;

upstream raw materials:

[1,2,4]oxadiazole-3-carboxylic acid hydrazide

Downstream raw materials:

2-(4-chloro-phenyl)-1-[1,2,4]oxadiazol-3-yl-2-(triphenyl-λ⁵-phosphanylidene)-ethanone

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