methyl((phenyl(pyridin-2-yl)methylene)quinolin-8-amino)platinum(II) perchlorate

Base Information

Chemical Name:methyl((phenyl(pyridin-2-yl)methylene)quinolin-8-amino)platinum(II) perchlorate
CAS No.:1313530-45-8
Molecular Formula:C₂₂H₁₈N₃Pt*ClO₄
Molecular Weight:618.936
Hs Code.:

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Technology Process of methyl((phenyl(pyridin-2-yl)methylene)quinolin-8-amino)platinum(II) perchlorate

There total 1 articles about methyl((phenyl(pyridin-2-yl)methylene)quinolin-8-amino)platinum(II) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 578-66-5
8-amino quinoline

: 91-02-1
phenyl(pyridin-2-yl)methanone

: chloromethyl(1,5-cyclooctadiene)platinum(II)

: lithium perchlorate

: 1313530-45-8
methyl((phenyl(pyridin-2-yl)methylene)quinolin-8-amino)platinum(II) perchlorate

Guidance literature:: In methanol; suspn. of Pt complex in CH3OH heated to 50°C, treated dropwise with 1 equiv. of 8-aminoquinoline and aldehyde in CH3OH, stirred at room temp. for 3 h, treated with 5:1 excess of LiClO4; kept at -25°C for 1 night, filtered, washed (CH3OH, Et2O), crystd.(Et2O diffusion into DMF/CH3NO2 soln.), elem. anal.;
DOI:10.1016/j.jorganchem.2011.03.046