Technology Process of C18H29N3O5S
There total 4 articles about C18H29N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C
2: formic acid / 20 °C
3: hydrogenchloride / methanol / 20 °C
With
hydrogenchloride; dmap; formic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane;
DOI:10.1016/j.bmcl.2013.01.038
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen bromide / acetonitrile; water / 0.08 h
1.2: 110 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C
3.1: formic acid / 20 °C
4.1: hydrogenchloride / methanol / 20 °C
With
hydrogenchloride; dmap; formic acid; hydrogen bromide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.038