C₁₄H₁₆F₃NO₅

Base Information

Chemical Name:C₁₄H₁₆F₃NO₅
CAS No.:1364927-40-1
Molecular Formula:C₁₄H₁₆F₃NO₅
Molecular Weight:335.28
Hs Code.:

C<sub>14</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>5</sub>

Synonyms:

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Chemical Property of C₁₄H₁₆F₃NO₅

Chemical Property:

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Technology Process of C₁₄H₁₆F₃NO₅

There total 9 articles about C₁₄H₁₆F₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₄₂F₃NO₆Si₂

: 1364927-40-1
C₁₄H₁₆F₃NO₅

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201102066

Reference yield:

: 1241725-14-3
C₁₇H₃₆O₃Si₂

: 1364927-40-1
C₁₄H₁₆F₃NO₅

Guidance literature:: Multi-step reaction with 7 steps

1: tributyl-amine; triphenyl-arsane; palladium diacetate / N,N-dimethyl-formamide / 15 h / 20 - 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3: sodium triacetoxyborohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

4: pyridine / 2.15 h / 20 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

6: triethylamine / dichloromethane / 0.33 h / 10 °C / Inert atmosphere

7: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With pyridine; tributyl-amine; triphenyl-arsane; palladium 10% on activated carbon; sodium triacetoxyborohydride; tetrabutyl ammonium fluoride; hydrogen; palladium diacetate; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1: Heck reaction;
DOI:10.1002/chem.201102066

Reference yield:

: C₂₁H₂₅NO₆

: 1364927-40-1
C₁₄H₁₆F₃NO₅

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 2.15 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 0.33 h / 10 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1002/chem.201102066