Technology Process of C18H19BrN2
There total 6 articles about C18H19BrN2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; thiophenol;
In
acetonitrile;
at 20 ℃;
for 16h;
DOI:10.1021/ja209836z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide; formic acid; acetic acid
2: sodium hydride / N,N-dimethyl-formamide
3: potassium carbonate; thiophenol / acetonitrile / 16 h / 20 °C
With
N-Bromosuccinimide; formic acid; sodium hydride; potassium carbonate; acetic acid; thiophenol;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja209836z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / dichloromethane
2: N-Bromosuccinimide; formic acid; acetic acid
3: sodium hydride / N,N-dimethyl-formamide
4: potassium carbonate; thiophenol / acetonitrile / 16 h / 20 °C
With
dmap; N-Bromosuccinimide; formic acid; sodium hydride; potassium carbonate; acetic acid; thiophenol; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja209836z