(M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

Base Information

Chemical Name:(M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester
CAS No.:145301-22-0
Molecular Formula:C₃₁H₃₁N₃O₇
Molecular Weight:557.603
Hs Code.:

(M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

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Chemical Property of (M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

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Technology Process of (M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

There total 5 articles about (M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 145301-13-9
(6R,6aS,8R,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7,8,11-hexahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

: 145301-22-0,145374-26-1
(M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

Guidance literature:: With hydrogenchloride; sodium nitrite; In ethanol; for 1h; Ambient temperature;
DOI:10.1002/ardp.19923251003

Reference yield:

: 141-97-9
ethyl acetoacetate

: 145301-22-0,145374-26-1
(M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / NH₄OAc, HOAc / 0.5 h / 90 - 100 °C

2: NaNO₂, conc. HCl / ethanol / 1 h / Ambient temperature

With hydrogenchloride; ammonium acetate; acetic acid; sodium nitrite; In ethanol;
DOI:10.1002/ardp.19923251003

Reference yield:

: 145301-06-0
(E)-(5R,9R,13S,14S)-(-)-4,5α-Epoxy-14-hydroxy-3-methoxy-17-methyl-7-(2-nitrobenzyliden)-morphinan-6-on

: 145301-22-0,145374-26-1
(M)-(6R,6aS,12R,12aS)-(-)-1,12-Epoxy-5,6,6a,7-tetrahydro-6a-hydroxy-6,12a-iminoethano-2-methoxy-10,15-dimethyl-8-(2-nitrophenyl)-(12H)-naphtho<2,1-g>chinolin-9-carbonsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / NH₄OAc, HOAc / 0.5 h / 90 - 100 °C

2: NaNO₂, conc. HCl / ethanol / 1 h / Ambient temperature

With hydrogenchloride; ammonium acetate; acetic acid; sodium nitrite; In ethanol;
DOI:10.1002/ardp.19923251003