Technology Process of C9H11N*C14H14O3
There total 7 articles about C9H11N*C14H14O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridinium chlorochromate / dichloromethane / 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / -40 °C
2.2: -40 °C
3.1: pyridinium chlorochromate / dichloromethane / 20 °C
4.1: water; lithium hydroxide / tetrahydrofuran / 4 h / 20 °C
5.1: diethyl ether
With
water; isopropylmagnesium chloride; pyridinium chlorochromate; lithium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/cjoc.201100083
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; lithium hydroxide / tetrahydrofuran / 4 h / 20 °C
2: diethyl ether
With
water; lithium hydroxide;
In
tetrahydrofuran; diethyl ether;
DOI:10.1002/cjoc.201100083
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -78 °C
1.2: -78 - 20 °C
1.3: Reflux
2.1: pyridinium chlorochromate / dichloromethane / 20 °C
3.1: isopropylmagnesium chloride / tetrahydrofuran / -40 °C
3.2: -40 °C
4.1: pyridinium chlorochromate / dichloromethane / 20 °C
5.1: water; lithium hydroxide / tetrahydrofuran / 4 h / 20 °C
6.1: diethyl ether
With
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; water; isopropylmagnesium chloride; pyridinium chlorochromate; lithium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/cjoc.201100083
