ap and sc(9S)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene

Base Information

Chemical Name:ap and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene
CAS No.:143838-65-7
Molecular Formula:C₃₀H₂₅Br
Molecular Weight:465.433
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ap and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene

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Technology Process of ap and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene

There total 2 articles about ap and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15540-91-7
2-amino-3,6-dimethylbenzoic acid

: 130927-57-0
1-Bromo-9-(2-methylbenzyl)anthracene

: 130927-56-9,130982-48-8,143838-65-7
ap and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene

Guidance literature:: With isopentyl nitrite; In acetone; for 0.25h; Heating;
DOI:10.1246/bcsj.65.1957

Reference yield:

: 87666-45-3
1-bromoanthracen-9(10H)-one

: 130927-56-9,130982-48-8,143838-65-7
ap and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene

Guidance literature:: Multi-step reaction with 2 steps

1: 2) SOCl₂, pyridine

2: 1) isopentyl nitrite / 2) acetone, reflux

With pyridine; thionyl chloride; isopentyl nitrite;
DOI:10.1246/cl.1990.1373