ClGe(ONCH(C₆H₅))Cr(CO)5

Base Information

Chemical Name:ClGe(ONCH(C₆H₅))Cr(CO)5
CAS No.:115775-73-0
Molecular Formula:C₁₂H₆ClCrGeNO₆
Molecular Weight:420.222
Hs Code.:

ClGe(ONCH(C<sub>6</sub>H<sub>5</sub>))Cr(CO)5

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Chemical Property of ClGe(ONCH(C₆H₅))Cr(CO)5

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Technology Process of ClGe(ONCH(C₆H₅))Cr(CO)5

There total 4 articles about ClGe(ONCH(C₆H₅))Cr(CO)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 115872-62-3
(C₂H₅)3GeONCH(C₆H₅)

: Cl₂GeCr(CO)5*C₄H₈O

: 115775-74-1
Ge(ONCH(C₆H₅))2Cr(CO)5

: 115775-73-0
ClGe(ONCH(C₆H₅))Cr(CO)5

Guidance literature:: In hexane; byproducts: Et3GeCl, THF; addn. of Et3GeONCHPh to suspn. of Cr complex in hexane, 1,5 h, ambient temp., molar ratio of educts Et3GeONCHPh:complex=2:1, stirred, sepn. of ppt., washed with hexane, dried in reduced pressure, Schlenk technique, under argon; elem. anal.;
DOI:10.1016/S0022-328X(00)98909-5

Reference yield: 86.0%

: 115872-62-3
(C₂H₅)3GeONCH(C₆H₅)

: Cl₂GeCr(CO)5*C₄H₈O

: 115775-73-0
ClGe(ONCH(C₆H₅))Cr(CO)5

Guidance literature:: In hexane; byproducts: Et3GeCl, THF; addn. of Et3GeONCHPh to suspn. of complex in hexane, 1,5 h, ambient temp., equimolar amts. of educts, stirred, sepn. of ppt., washed with hexane, dried in reduced pressure, Schlenk technique, under argon; elem. anal.;
DOI:10.1016/S0022-328X(00)98909-5

Reference yield: 77.0%

: 4149-28-4
bis(triethylgermyl)mercury

: Cl₂GeCr(CO)5*(C₆H₅)CHNOH

: 115775-73-0
ClGe(ONCH(C₆H₅))Cr(CO)5

Guidance literature:: In benzene; byproducts: Et3GeH, Et3GeCl, Hg; addn. of (Et3Ge)2Hg to soln. of complex in benzene, 12h, 20°C, stirred, darkness, sepn. of Hg, evapn. in reduced pressure, pptn. by addn. of pentane/ether, drying, under argon; identified by IR, MS and (1)H-NMR;
DOI:10.1016/S0022-328X(00)98909-5