Technology Process of C25H39NPPd(1+)*CF3O3S(1-)
There total 5 articles about C25H39NPPd(1+)*CF3O3S(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: activated 4 ? molecular sieves / pentane / 96 h / 0 °C
2: diethyl ether / 3 h / 20 °C / Schlenk technique
3: dichloromethane / 14 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox
4: dichloromethane / 14 h / Darkness; Inert atmosphere; Schlenk technique; Glovebox
With
activated 4 ? molecular sieves;
In
diethyl ether; dichloromethane; pentane;
DOI:10.1021/om301102w
- Guidance literature:
-
Multi-step reaction with 4 steps
1: activated 4 ? molecular sieves / pentane / 96 h / 0 °C
2: diethyl ether / 3 h / 20 °C / Schlenk technique
3: dichloromethane / 14 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox
4: dichloromethane / 14 h / Darkness; Inert atmosphere; Schlenk technique; Glovebox
With
activated 4 ? molecular sieves;
In
diethyl ether; dichloromethane; pentane;
DOI:10.1021/om301102w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethyl ether / 3 h / 20 °C / Schlenk technique
2: dichloromethane / 14 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox
3: dichloromethane / 14 h / Darkness; Inert atmosphere; Schlenk technique; Glovebox
In
diethyl ether; dichloromethane;
DOI:10.1021/om301102w