N-Diallylamino-diphenyl-phosphin

Base Information

Chemical Name:N-Diallylamino-diphenyl-phosphin
CAS No.:94066-97-4
Molecular Formula:C₁₈H₂₀NP
Molecular Weight:281.337
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Diallylamino-diphenyl-phosphin

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Technology Process of N-Diallylamino-diphenyl-phosphin

There total 1 articles about N-Diallylamino-diphenyl-phosphin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94066-97-4
N-Diallylamino-diphenyl-phosphin

Guidance literature:: Eintr. einer Lsg. v. Diphenylchlorphosphin in Bzl. in Lsg. v. Diallylamin in Bzl. bei 0-5grad (0.5h);
DOI:10.1021/jo01061a617

Reference yield: 96.0%

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 94066-97-4
N-Diallylamino-diphenyl-phosphin

: 827346-07-6
[RhCl((C₆H₅)2PN(CH₂CHCH₂)2)2]

Guidance literature:: In dichloromethane; ligand and Rh compd. dissolved in CH2Cl2; concd.; pptd. with Et2O, filtered; elem. anal.;
DOI:10.1016/j.poly.2004.09.017

Reference yield: 92.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 94066-97-4
N-Diallylamino-diphenyl-phosphin

: Pd⁽²⁺⁾*2Cl^(1-)*2(C₆H₅)2PN(CH₂CHCH₂)2=[PdCl₂((C₆H₅)2PN(CH₂CHCH₂)2)2]

Guidance literature:: In dichloromethane; 3 equiv. of ligand and Pd compd. dissolved in CH2Cl2 and strirred for 30min; concd.; pptd. with Et2O, filtered; elem. anal.;
DOI:10.1016/j.poly.2004.09.017