8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside
CAS No.:73991-11-4
Molecular Formula:C₅₇H₇₁NO₂₁
Molecular Weight:1106.18
Hs Code.:

8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Synonyms:

Suppliers and Price of 8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

There total 5 articles about 8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 73983-02-5
8-methoxycarbonyloctyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

: 5158-64-5
2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl bromide

: 73991-11-4
8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; 1.) 8 h, 2.) overnight;
DOI:10.1016/S0008-6215(00)85316-1

Reference yield: 45.0%

: 73983-02-5
8-methoxycarbonyloctyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

: 5160-09-8
2,3,4‐tri‐O‐acetyl-α-L‐rhamnopyranosyl chloride

: 73991-11-4
8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; 1.) 8 h, 2.) overnight, -70 deg C to RT;
DOI:10.1016/S0008-6215(00)85316-1

Reference yield:

: 70801-92-2,82863-55-6,82950-99-0,146276-05-3
8-methoxycarbonyloctyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

: 73991-11-4
8-methoxycarbonyloctyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)-O-(2,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glycopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Na / methanol

2: 1.) trimethyl orthobenzoate, p-toluenesulphonic acid; 2.) pyridine / 1.) DMF, 20 h, RT; 2.) chloroform, 0 deg C, overnight

3: 45 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂ / 1.) 8 h, 2.) overnight, -70 deg C to RT

With pyridine; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; tetramethylurea; orthobenzoic acid trimethyl ester; sodium; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)85316-1