Technology Process of C47H60BrNO2Si2
There total 8 articles about C47H60BrNO2Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: palladium on activated charcoal; hydrogen / 2625.26 Torr
2: acetic acid / water
3: dmap; pyridine
4: lithium aluminium tetrahydride / tetrahydrofuran
5: triethylamine
6: lithium bromide
With
pyridine; dmap; lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; acetic acid; triethylamine; lithium bromide;
In
tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2013.01.022
- Guidance literature:
-
Multi-step reaction with 7 steps
1: toluene-4-sulfonic acid
2: palladium on activated charcoal; hydrogen / 2625.26 Torr
3: acetic acid / water
4: dmap; pyridine
5: lithium aluminium tetrahydride / tetrahydrofuran
6: triethylamine
7: lithium bromide
With
pyridine; dmap; lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; acetic acid; triethylamine; lithium bromide;
In
tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2013.01.022
- Guidance literature:
-
Multi-step reaction with 8 steps
1: nitric acid
2: toluene-4-sulfonic acid
3: palladium on activated charcoal; hydrogen / 2625.26 Torr
4: acetic acid / water
5: dmap; pyridine
6: lithium aluminium tetrahydride / tetrahydrofuran
7: triethylamine
8: lithium bromide
With
pyridine; dmap; lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; nitric acid; toluene-4-sulfonic acid; acetic acid; triethylamine; lithium bromide;
In
tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2013.01.022