1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine

Base Information

Chemical Name:1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine
CAS No.:99602-51-4
Molecular Formula:C₁₄H₁₄N₄O₅
Molecular Weight:318.289
Hs Code.:

1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopenta<c>pyradizine

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Suppliers and Price of 1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine

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Technology Process of 1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine

There total 2 articles about 1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 344557-42-2
2-chloro-1-(2,4-dinitrophenylazo)ethene

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 99602-51-4
1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine

Guidance literature:: In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: 19072-93-6
dichloroacetaldehyde 2,4-dinitrophenylhydrazone

: 99602-51-4
1-(2,4-dinitrophenyl)-4-methoxy-4,4a,5,7a-tetrahydro-1H-cyclopentapyradizine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / anhydrous sodium carbonate / CH₂Cl₂ / 24 h / Ambient temperature

2: 16 percent / CH₂Cl₂ / 20 h / 20 °C

With sodium carbonate; In dichloromethane;