Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Base Information

Chemical Name:Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid
CAS No.:87591-32-0
Molecular Formula:C₇₃H₇₂N₂O₁₃
Molecular Weight:1185.38
Hs Code.:

Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

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Chemical Property of Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

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Technology Process of Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

There total 10 articles about Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 673-22-3
2-Hydroxy-4-methoxybenzaldehyde

: 87591-31-9
Phenyl-O-<4-O-(5-aminopyridin-2-yl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

: 87591-32-0
Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Guidance literature:: In methanol; for 0.166667h; Heating;

Reference yield:

: 100-44-7
benzyl chloride

: 87591-32-0
Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 47 percent / KOH / dioxane / 7 h / Heating

2: 79 percent / NaH / benzene / 72 h / Heating

3: 61 percent / 0.5 M aq. HCl / dioxane / 4 h / Heating

4: 84 percent / NaH / 4 h / Ambient temperature

5: 91 percent / NaH / dimethylsulfoxide / 20 h / Ambient temperature

6: 37 percent / Raney nickel, H₂ / ethyl acetate; methanol / Ambient temperature; 1) 5 d, 2) 24 h

7: 62 percent / methanol / 0.17 h / Heating

With hydrogenchloride; potassium hydroxide; hydrogen; nickel; sodium hydride; In 1,4-dioxane; methanol; dimethyl sulfoxide; ethyl acetate; benzene;

Reference yield:

: 55287-35-9,55287-36-0,87638-63-9
(2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

: 87591-32-0
Phenyl-O-<2,3,6-tri-O-benzyl-4-O-<5-(2-hydroxy-4-methoxybenzylidenamino)-2-pyridinyl>-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 47 percent / KOH / dioxane / 7 h / Heating

2: 79 percent / NaH / benzene / 72 h / Heating

3: 61 percent / 0.5 M aq. HCl / dioxane / 4 h / Heating

4: 84 percent / NaH / 4 h / Ambient temperature

5: 91 percent / NaH / dimethylsulfoxide / 20 h / Ambient temperature

6: 37 percent / Raney nickel, H₂ / ethyl acetate; methanol / Ambient temperature; 1) 5 d, 2) 24 h

7: 62 percent / methanol / 0.17 h / Heating

With hydrogenchloride; potassium hydroxide; hydrogen; nickel; sodium hydride; In 1,4-dioxane; methanol; dimethyl sulfoxide; ethyl acetate; benzene;