C₅₉H₁₀₂O₁₅Si₃

Base Information

• Chemical Name: C₅₉H₁₀₂O₁₅Si₃
• CAS No.: 145095-79-0
• Molecular Formula: C₅₉H₁₀₂O₁₅Si₃
• Molecular Weight: 1135.71
• Mol file: 145095-79-0.mol

Synonyms:

Chemical Property of C₅₉H₁₀₂O₁₅Si₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₁₀₂O₁₅Si₃

There total 5 articles about C₅₉H₁₀₂O₁₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C68H120O18Si3 (141243-00-7) → C59H102O15Si3 (145095-79-0)

Guidance literature:

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(00)91896-3

Reference yield:

C63H108O16Si3 (131077-76-4,145165-15-7) → C59H102O15Si3 (145095-79-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 95 percent / Pb(OAc)4, pyridine

2: LiCl, diisopropylethylamine / acetonitrile / Ambient temperature

3: Na₂S₂O₃, NaHCO₃ / benzene; H₂O / Heating

4: 100 percent / sodium borohydride / methanol / Ambient temperature

5: pyridinium p-toluenesulfonate, p-toluenesulfonic acid / CH₂Cl₂ / Ambient temperature

With pyridine; lead(IV) acetate; sodium tetrahydroborate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; toluene-4-sulfonic acid; sodium thiosulfate; N-ethyl-N,N-diisopropylamine; lithium chloride; In methanol; dichloromethane; water; acetonitrile; benzene;

DOI:10.1016/S0040-4039(00)91896-3

Reference yield:

C64H110O17Si3 (141242-63-9) → C59H102O15Si3 (145095-79-0)

Guidance literature:

Multi-step reaction with 4 steps

1: LiCl, diisopropylethylamine / acetonitrile / Ambient temperature

2: Na₂S₂O₃, NaHCO₃ / benzene; H₂O / Heating

3: 100 percent / sodium borohydride / methanol / Ambient temperature

4: pyridinium p-toluenesulfonate, p-toluenesulfonic acid / CH₂Cl₂ / Ambient temperature

With sodium tetrahydroborate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; toluene-4-sulfonic acid; sodium thiosulfate; N-ethyl-N,N-diisopropylamine; lithium chloride; In methanol; dichloromethane; water; acetonitrile; benzene;

DOI:10.1016/S0040-4039(00)91896-3

upstream raw materials:

C₆₈H₁₂₀O₁₈Si₃

C₆₃H₁₀₈O₁₆Si₃

C₆₄H₁₁₀O₁₇Si₃

C₆₈H₁₁₈O₁₈Si₃