Technology Process of C41H75NO10Si2
There total 5 articles about C41H75NO10Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate;
In
dichloromethane; toluene;
at 0 - 20 ℃;
for 20h;
stereoselective reaction;
Molecular sieve;
DOI:10.1021/ml300230h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C
1.2: 7 h / -45 - 20 °C
2.1: camphor-10-sulfonic acid / methanol / 1 h / 0 °C
3.1: 1H-imidazole / dichloromethane / 3 h / 20 °C
4.1: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; toluene / 20 h / 0 - 20 °C / Molecular sieve
With
1H-imidazole; n-butyllithium; 2,6-di-tert-butyl-4-methylpyridine; camphor-10-sulfonic acid; silver trifluoromethanesulfonate;
In
tetrahydrofuran; methanol; hexane; dichloromethane; toluene;
DOI:10.1021/ml300230h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1H-imidazole / dichloromethane / 3 h / 20 °C
2: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; toluene / 20 h / 0 - 20 °C / Molecular sieve
With
1H-imidazole; 2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate;
In
dichloromethane; toluene;
DOI:10.1021/ml300230h
