(3R)-3-Hydroxy-β-jonon-trisylhydrazon

Base Information

Chemical Name:(3R)-3-Hydroxy-β-jonon-trisylhydrazon
CAS No.:87162-51-4
Molecular Formula:C₂₈H₄₄N₂O₃S
Molecular Weight:488.735
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R)-3-Hydroxy-β-jonon-trisylhydrazon

Chemical Property:

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Technology Process of (3R)-3-Hydroxy-β-jonon-trisylhydrazon

There total 1 articles about (3R)-3-Hydroxy-β-jonon-trisylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39085-59-1
trisylhydrazine

: 50281-38-4
(3R)-3-hydroxy-β-ionone

: 87162-51-4
(3R)-3-Hydroxy-β-jonon-trisylhydrazon

Guidance literature:: In diethyl ether; for 12h; Ambient temperature;
DOI:10.1002/hlca.19830660418

Reference yield:

: 87162-51-4
(3R)-3-Hydroxy-β-jonon-trisylhydrazon

: (3R,6'R)-β,ε-Carotin-3,19-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) TMEDA, 15percent BuLi / 1.) hexane; 2.) hexane, 15 min, 0 deg C

2: 274 mg / 1 N H₂SO₄ / acetone; tetrahydrofuran / 20 h / Ambient temperature

3: hydrogen / Lindlar catalyst / ethyl acetate; quinoline / 1.5 h

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; hydrogen; Lindlar's catalyst; In tetrahydrofuran; quinoline; ethyl acetate; acetone;
DOI:10.1002/hlca.19830660418

Reference yield:

: 87162-51-4
(3R)-3-Hydroxy-β-jonon-trisylhydrazon

: (-)-(1R)-4-(1',3'-Butadienyl)-3,5,5-trimethyl-3-cyclohexen-1-ol

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; for 17h; Ambient temperature;
DOI:10.1002/hlca.19830660418