Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester

Base Information

Chemical Name:Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester
CAS No.:144368-16-1
Molecular Formula:C₂₃H₃₄O₄
Molecular Weight:374.521
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester

Chemical Property:

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Technology Process of Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester

There total 10 articles about Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144368-18-3
1-bromo-tetradec-3-yne

: 144368-16-1
Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) MgBr / 1.) ether

2: Lindlar reduction

3: metachloroperbenzoic acid / CH₂Cl₂

4: AcOH / CH₂Cl₂ / 12 h / 20 °C

5: benzoylation

6: H₂ / Pd/C

7: aq. HOAc / 40 °C

8: NaIO₄ / H₂O / 20 °C

9: OH^(1-) , H₂O

With sodium periodate; water; hydroxide; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; palladium on activated charcoal; In dichloromethane; water;
DOI:10.1016/S0040-4039(00)79126-X

Reference yield:

: Toluene-4-sulfonic acid tetradec-3-ynyl ester

: 144368-16-1
Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: MgBr / diethyl ether

2: 1.) MgBr / 1.) ether

3: Lindlar reduction

4: metachloroperbenzoic acid / CH₂Cl₂

5: AcOH / CH₂Cl₂ / 12 h / 20 °C

6: benzoylation

7: H₂ / Pd/C

8: aq. HOAc / 40 °C

9: NaIO₄ / H₂O / 20 °C

10: OH^(1-) , H₂O

With sodium periodate; water; hydroxide; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; palladium on activated charcoal; In diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4039(00)79126-X

Reference yield:

: 144368-09-2
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-(tridec-(2'Z)-enyl)-β-L-idofuranose

: 144368-16-1
Benzoic acid (S)-1-((2S,5S)-5-formyl-tetrahydro-furan-2-yl)-undecyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: metachloroperbenzoic acid / CH₂Cl₂

2: AcOH / CH₂Cl₂ / 12 h / 20 °C

3: benzoylation

4: H₂ / Pd/C

5: aq. HOAc / 40 °C

6: NaIO₄ / H₂O / 20 °C

7: OH^(1-) , H₂O

With sodium periodate; water; hydroxide; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; water;
DOI:10.1016/S0040-4039(00)79126-X