C₁₅H₂₃NO₄

Base Information

Chemical Name:C₁₅H₂₃NO₄
CAS No.:1438281-13-0
Molecular Formula:C₁₅H₂₃NO₄
Molecular Weight:281.352
Hs Code.:

C<sub>15</sub>H<sub>23</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₅H₂₃NO₄

There total 6 articles about C₁₅H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1438281-08-3
C₁₅H₁₉NO₄

: 1438281-13-0
C₁₅H₂₃NO₄

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: hydrogen; palladium hydroxide 10 wt. % on activated carbon / methanol / 7 h / 760.05 Torr

4: dichloromethane / 15 h / 20 °C / Inert atmosphere

5: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 5 h / 100 °C / Inert atmosphere

6: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; dimethylsulfide borane complex; palladium hydroxide 10 wt. % on activated carbon; hydrogen; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; toluene; 5: |Mitsunobu Displacement;
DOI:10.1039/c3ob27390c

Reference yield:

: 1438281-07-2
C₁₅H₁₇NO₃

: 1438281-13-0
C₁₅H₂₃NO₄

Guidance literature:: Multi-step reaction with 7 steps

1: trifluoroacetic acid / tetrahydrofuran; water / 15 h / Inert atmosphere

2: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

4: hydrogen; palladium hydroxide 10 wt. % on activated carbon / methanol / 7 h / 760.05 Torr

5: dichloromethane / 15 h / 20 °C / Inert atmosphere

6: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 5 h / 100 °C / Inert atmosphere

7: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; dimethylsulfide borane complex; palladium hydroxide 10 wt. % on activated carbon; hydrogen; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 6: |Mitsunobu Displacement;
DOI:10.1039/c3ob27390c

Reference yield:

: 1438281-11-8
C₇H₁₅NO₄

: 1438281-13-0
C₁₅H₂₃NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 15 h / 20 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 5 h / 100 °C / Inert atmosphere

3: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; dimethylsulfide borane complex; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; 2: |Mitsunobu Displacement;
DOI:10.1039/c3ob27390c