C₃₀H₃₃NO₂

Base Information

Chemical Name:C₃₀H₃₃NO₂
CAS No.:1448055-14-8
Molecular Formula:C₃₀H₃₃NO₂
Molecular Weight:439.598
Hs Code.:

C<sub>30</sub>H<sub>33</sub>NO<sub>2</sub>

Synonyms:

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Chemical Property of C₃₀H₃₃NO₂

Chemical Property:

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Technology Process of C₃₀H₃₃NO₂

There total 4 articles about C₃₀H₃₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (Z)-3'-phenylprop-2'-en-1'-yl (3R,αS,E)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate

: 1448055-13-7
C₃₀H₃₃NO₂

: 1448055-14-8
C₃₀H₃₃NO₂

Guidance literature:: (Z)-3'-phenylprop-2'-en-1'-yl (3R,αS,E)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate; With chloro-trimethyl-silane; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.25h;

In tetrahydrofuran; toluene; for 1h; Overall yield = 2 g; Reflux;
DOI:10.1039/c3cc43250e

Reference yield:

: 1448055-07-9
tert-butyl (3R,αS,E)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate

: 1448055-13-7
C₃₀H₃₃NO₂

: 1448055-14-8
C₃₀H₃₃NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 - 20 °C

2.2: 0 - 20 °C

3.1: chloro-trimethyl-silane; lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C

3.2: 1 h / Reflux

With chloro-trimethyl-silane; oxalyl dichloride; N,N-dimethyl-formamide; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene; 3.2: |Claisen-Ireland Rearrangement;
DOI:10.1039/c3cc43250e

Reference yield:

: 110-44-1,91751-55-2
sorbic Acid

: 1448055-13-7
C₃₀H₃₃NO₂

: 1448055-14-8
C₃₀H₃₃NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: Acidic conditions

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 - 20 °C

4.2: 0 - 20 °C

5.1: chloro-trimethyl-silane; lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C

5.2: 1 h / Reflux

With n-butyllithium; chloro-trimethyl-silane; oxalyl dichloride; N,N-dimethyl-formamide; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; toluene; 5.2: |Claisen-Ireland Rearrangement;
DOI:10.1039/c3cc43250e