Technology Process of 4-nitrophenyl 2,3,6-tri-O-acetyl-4-deoxy-β-D-lyxo-hexopyranoside
There total 3 articles about 4-nitrophenyl 2,3,6-tri-O-acetyl-4-deoxy-β-D-lyxo-hexopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 62 percent / silver(I)carbonate, calcium sulphate / acetone / 3 h / Ambient temperature
2: 1.) phosphorus(V)oxide; 2.) sodium borohydride; 3.) pyridine / 1.) dimethyl sulfoxide, N,N-dimethylformamide 2 h, 65-70 deg C; 2.) methanol, 30 min; 3.) 16 h, RT
With
pyridine; phosphorus pentaoxide; calcium sulfate; sodium tetrahydroborate; silver carbonate;
In
acetone;
DOI:10.1016/0008-6215(83)84067-1
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 62 percent / silver(I)carbonate, calcium sulphate / acetone / 3 h / Ambient temperature
2: 1.) phosphorus(V)oxide; 2.) sodium borohydride; 3.) pyridine / 1.) dimethyl sulfoxide, N,N-dimethylformamide 2 h, 65-70 deg C; 2.) methanol, 30 min; 3.) 16 h, RT
With
pyridine; phosphorus pentaoxide; calcium sulfate; sodium tetrahydroborate; silver carbonate;
In
acetone;
DOI:10.1016/0008-6215(83)84067-1
- Guidance literature:
-
With
pyridine; phosphorus pentaoxide; sodium tetrahydroborate;
Yield given. Multistep reaction;
1.) dimethyl sulfoxide, N,N-dimethylformamide 2 h, 65-70 deg C; 2.) methanol, 30 min; 3.) 16 h, RT;
DOI:10.1016/0008-6215(83)84067-1
