12-[3-O-(Bromoacetyl)-4-O-methyl-beta-D-glucopyranosyl]-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Base Information

• Chemical Name: 12-[3-O-(Bromoacetyl)-4-O-methyl-beta-D-glucopyranosyl]-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione
• CAS No.: 220726-77-2
• Molecular Formula: C₂₉H₂₄BrN₃O₈
• Molecular Weight: 622.429
• Mol file: 220726-77-2.mol

Synonyms:

Chemical Property of 12-[3-O-(Bromoacetyl)-4-O-methyl-beta-D-glucopyranosyl]-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 12-[3-O-(Bromoacetyl)-4-O-methyl-beta-D-glucopyranosyl]-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

There total 1 articles about 12-[3-O-(Bromoacetyl)-4-O-methyl-beta-D-glucopyranosyl]-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromoacetyl bromide (598-21-0) + 5H-indolo(2,3-a)pyrrolo(3,4-c)carbazole-5,7(6h)-dione,1,11-dichloro-12,13-dihydro-12-(4-omethyl-beta-d-glucopyranosyl) (205386-72-7) → 12-(2-O-bromomethylcarbonyl-4-O-methyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo<2,3-a>pyrrolo<3,4-c>carbazole-5,7-dione + 12-(3-O-bromomethylcarbonyl-4-O-methyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo<2,3-a>pyrrolo<3,4-c>carbazole-5,7-dione (220726-77-2)

Guidance literature:

With potassium tert-butylate; Yield given; Multistep reaction. Yields of byproduct given; 1.) THF, RT, 0.5 h, 2.) THF, RT, 24 h;

DOI:10.1021/jm980396d

upstream raw materials:

2-Bromoacetyl bromide

5H-indolo(2,3-a)pyrrolo(3,4-c)carbazole-5,7(6h)-dione,1,11-dichloro-12,13-dihydro-12-(4-omethyl-beta-d-glucopyranosyl)