3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate)

Base Information

• Chemical Name: 3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate)
• CAS No.: 134662-27-4
• Molecular Formula: C₆H₁₅N*C₁₂₂H₁₃₄NO₂₆P
• Molecular Weight: 2162.56

Synonyms:

Chemical Property of 3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate)

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Technology Process of 3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate)

There total 1 articles about 3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylamine carbonate (15715-58-9) + 3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-α,β-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl phosphonate) (134662-25-2,134732-31-3,134732-34-6,134732-35-7) → 3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate) (134662-27-4,134732-33-5)

Guidance literature:

With iodine; Yield given. Multistep reaction; 1) THF, H₂O, pyridine, 3 h, 2) CH₂Cl₂;

DOI:10.1016/0008-6215(91)80096-6

Reference yield:

3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-Glcp)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-Galp>-αβ-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl triethylammonium phosphate) (134662-27-4,134732-33-5) → 3-aminopropyl 4-O-(4-O-β-D-glucopyranosyl-2-O-α-L-rhamnopyranosyl-β-D-galactopyranosyl)-α-L-rhamnopyranoside 3'-(glycer-2-yl sodium phosphate) (143873-66-9) + 3-aminopropyl 4-O-(4-O-β-D-glucopyranosyl-2-O-α-L-rhamnopyranosyl-β-D-galactopyranosyl)-β-L-rhamnopyranoside 3'-(glycer-2-yl sodium phosphate) (143873-66-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; isopropyl alcohol; for 48h;

DOI:10.1016/0008-6215(91)80096-6

upstream raw materials:

triethylamine carbonate

3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-α,β-L-rhamnopyranoside 3'-(1,3-di-O-benzylglycer-2-yl phosphonate)

Downstream raw materials:

3-aminopropyl 4-O-(4-O-β-D-glucopyranosyl-2-O-α-L-rhamnopyranosyl-β-D-galactopyranosyl)-α-L-rhamnopyranoside 3'-(glycer-2-yl sodium phosphate)

3-aminopropyl 4-O-(4-O-β-D-glucopyranosyl-2-O-α-L-rhamnopyranosyl-β-D-galactopyranosyl)-β-L-rhamnopyranoside 3'-(glycer-2-yl sodium phosphate)

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