3-phenylpropyl α-disulfone

Base Information

• Chemical Name: 3-phenylpropyl α-disulfone
• CAS No.: 77357-66-5
• Molecular Formula: C₁₈H₂₂O₄S₂
• Molecular Weight: 366.502
• Mol file: 77357-66-5.mol

Synonyms:

Chemical Property of 3-phenylpropyl α-disulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-phenylpropyl α-disulfone

There total 2 articles about 3-phenylpropyl α-disulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

3-phenyl-propane-1-sulfinic acid (70385-57-8) → 3-phenylpropyl α-disulfone (77357-66-5)

Guidance literature:

With cobalt(II) sulfate;

DOI:10.1021/jo00325a040

Reference yield:

1-Bromo-3-phenylpropane (637-59-2) → 3-phenylpropyl α-disulfone (77357-66-5)

Guidance literature:

Multi-step reaction with 2 steps

2: 19 percent / acidic cobaltic sulfate

With cobalt(II) sulfate;

DOI:10.1021/jo00325a040

Reference yield:

3-phenylpropyl α-disulfone (77357-66-5) → C9H11O2S

Guidance literature:

In various solvent(s); at 133.8 ℃; Rate constant; Kinetics; Thermodynamic data; diff. temp.; ΔH(excit.), ΔS(excit.);

DOI:10.1021/jo00325a040

upstream raw materials:

3-phenyl-propane-1-sulfinic acid

1-Bromo-3-phenylpropane