C₆H₄C₂H₄(OSi(CH₃)3)2C₁₀H₅O₂(C₃H₄O₂(CH₃))O₂BC₆H₅

Base Information

• Chemical Name: C₆H₄C₂H₄(OSi(CH₃)3)2C₁₀H₅O₂(C₃H₄O₂(CH₃))O₂BC₆H₅
• CAS No.: 262417-81-2
• Molecular Formula: C₃₄H₄₃BO₈Si₂
• Molecular Weight: 646.693
• Mol file: 262417-81-2.mol

Synonyms:

Chemical Property of C₆H₄C₂H₄(OSi(CH₃)3)2C₁₀H₅O₂(C₃H₄O₂(CH₃))O₂BC₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₆H₄C₂H₄(OSi(CH₃)3)2C₁₀H₅O₂(C₃H₄O₂(CH₃))O₂BC₆H₅

There total 1 articles about C₆H₄C₂H₄(OSi(CH₃)3)2C₁₀H₅O₂(C₃H₄O₂(CH₃))O₂BC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-bis(trimethylsilyloxy)benzocyclobutene + C10H7O2(C3H4O2(CH3))O2BC6H5 + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → C6H4C2H4(OSi(CH3)3)2C10H5O2(C3H4O2(CH3))O2BC6H5 (262417-81-2)

Guidance literature:

In tetrahydrofuran; ⁽²⁾H₈-toluene; 45 °C for 7 h, solvent was removed, residue was taken up in THF, solid DDQ was added, stirred for 12 h at 25 °C; soln. was diluted with CH2Cl2, washed twice with satd. NaHCO3 soln., dried over Na2SO4, solvent was removed by evapn.;

DOI:10.1021/ja993627u

upstream raw materials:

2,3-dicyano-5,6-dichloro-p-benzoquinone

Refernces