1-phenyl-3-ruthenocenylpropane-1,3-dione

Base Information

Chemical Name:1-phenyl-3-ruthenocenylpropane-1,3-dione
CAS No.:436141-56-9
Molecular Formula:C₁₉H₁₆O₂Ru
Molecular Weight:377.405
Hs Code.:

Synonyms:

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Chemical Property of 1-phenyl-3-ruthenocenylpropane-1,3-dione

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Technology Process of 1-phenyl-3-ruthenocenylpropane-1,3-dione

There total 3 articles about 1-phenyl-3-ruthenocenylpropane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 1-ruthenocenylethan-1-one

: 1-phenyl-3-ruthenocenylpropane-1,3-dione

: 436141-56-9
1-phenyl-3-ruthenocenylpropane-1,3-dione

Guidance literature:: With lithium diisopropylamide; In tetrahydrofuran; soln. of amide was added to soln. of Ru complex in THF; stirred for 20 min while cooled on ice; ester was added; stirred at room temp. for 16 h; ether added; filtered; ice-cold HCl soln. added; stirred for 5 min; extd. (ether); org. layer washed (H2O); dried (MgSO4); filtered; evapd. (vac.); chromd. (Kieselgel, ether/hexane, 2/1);
DOI:10.1021/om700609z

Reference yield:

: 1-phenyl-3-ruthenocenylpropane-1,3-dione

: 436141-56-9
1-phenyl-3-ruthenocenylpropane-1,3-dione

Guidance literature:: In chloroform-d1; Ru complex was dissolved in CDCl3 at 293 K; NMR monitoring; Kinetics;
DOI:10.1021/om700609z

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 1-ruthenocenylethan-1-one

: 436141-56-9
1-phenyl-3-ruthenocenylpropane-1,3-dione

Guidance literature:: 1-ruthenocenylethan-1-one; With lithium diisopropyl amide; In tetrahydrofuran; at 20 ℃; for 0.5h; Cooling with ice; Schlenk technique;

benzoic acid methyl ester; In tetrahydrofuran; at 20 ℃; for 16h; Kinetics; Cooling with ice; Schlenk technique;
DOI:10.1039/c3nj00354j