tetrahydrothiophen-3-one oxime

Base Information

• Chemical Name: tetrahydrothiophen-3-one oxime
• CAS No.: 128862-26-0
• Molecular Formula: C₄H₇NOS
• Molecular Weight: 117.172
• Mol file: 128862-26-0.mol

Synonyms:

Chemical Property of tetrahydrothiophen-3-one oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tetrahydrothiophen-3-one oxime

There total 1 articles about tetrahydrothiophen-3-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Tetrahydrothiophen-3-one (1003-04-9) → tetrahydrothiophen-3-one oxime (128862-26-0)

Guidance literature:

With hydroxylamine hydrochloride; barium carbonate; In ethanol; for 2.5h; Heating;

Reference yield: 57.0%

tetrahydrothiophen-3-one oxime (128862-26-0) → 3-Thiacyclopentylamin (101993-01-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1002/ardp.19903230512

upstream raw materials:

Tetrahydrothiophen-3-one

Downstream raw materials:

3-Thiacyclopentylamin

Refernces

• 1、 Grigg,Heaney,Surendrakumar,Warnock. "X=Y-ZH systems as potentials 1,3-dipoles. Part 321,2 generation of nitrones from oximes. Tandem Michael addition-1,3-dipolar cycloaddition reactions. Background and class 1 processes". . p. 4477 - 4494. Retrieved 2007/10/02.