1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline

Base Information

Chemical Name:1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline
CAS No.:78375-91-4
Molecular Formula:C₁₇H₂₉N₃O₃
Molecular Weight:323.436
Hs Code.:

1,3-dihydroxy-2-<p-(N-t-butylhydroxylamino)phenyl>-4,4,5,5-tetramethyl-2-imidazoline

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline

Chemical Property:

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Technology Process of 1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline

There total 5 articles about 1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 23819-68-3
N-t-butyl-N-(p-formylphenyl)hydroxylamine

: 78375-91-4
1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline

Guidance literature:: With sodium carbonate; In ethanol; for 18h; Heating;
DOI:10.1039/P19810001165

Reference yield:

: 96259-22-2
4-methoxymethylphenylmagnesium bromide

: 78375-91-4
1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / tetrahydrofuran; diethyl ether / 0.5 h

2: 69 percent / silver oxide, magnesium sulphate / benzene

3: 38 percent / sodium carbonate / ethanol / 18 h / Heating

With sodium carbonate; magnesium sulfate; silver(l) oxide; In tetrahydrofuran; diethyl ether; ethanol; benzene;
DOI:10.1039/P19810001165

Reference yield:

: 78375-79-8
N-t-butyl-N-(p-methoxymethylphenyl)hydroxylamine

: 78375-91-4
1,3-dihydroxy-2--4,4,5,5-tetramethyl-2-imidazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / silver oxide, magnesium sulphate / benzene

2: 38 percent / sodium carbonate / ethanol / 18 h / Heating

With sodium carbonate; magnesium sulfate; silver(l) oxide; In ethanol; benzene;
DOI:10.1039/P19810001165