Technology Process of C32H24O2
There total 13 articles about C32H24O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 12 steps
1: Pd(PPh3)4; CuI / triethylamine / 20 °C
2: imidazole / CH2Cl2
3: 93 percent / NaBH4 / methanol; CH2Cl2
4: 99 percent / hydrogen / Lindlar / benzene; quinoline
5: 98 percent / Dess-Martin / CH2Cl2
6: 92 percent / VCl3(THF)3; Zn / CH2Cl2 / 20 °C
7: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C
8: NaBH4 / methanol; CH2Cl2
9: 94 percent / 4-dimethylaminopyridine / CH2Cl2 / 0 °C
10: 83 percent / 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine / benzene / Heating
11: n-Bu4NF / tetrahydrofuran
12: Dess-Martin / CH2Cl2
With
1H-imidazole; 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine; dmap; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); oxalyl dichloride; Vanadium (III) chloride-(tris-tetrahydrofuran); tetrabutyl ammonium fluoride; hydrogen; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; zinc;
Lindlar's catalyst;
In
tetrahydrofuran; quinoline; methanol; dichloromethane; triethylamine; benzene;
1: Arylation / 2: Etherification / 3: Reduction / 4: Catalytic hydrogenation / 5: Oxidation / 6: Dimerization / 7: Oxidation / 8: Reduction / 9: thiocarbonylation / 10: reductive dehydroxylation / 11: desilylation / 12: Oxidation;
DOI:10.1016/S0040-4039(99)02062-6
- Guidance literature:
-
Multi-step reaction with 11 steps
1: imidazole / CH2Cl2
2: 93 percent / NaBH4 / methanol; CH2Cl2
3: 99 percent / hydrogen / Lindlar / benzene; quinoline
4: 98 percent / Dess-Martin / CH2Cl2
5: 92 percent / VCl3(THF)3; Zn / CH2Cl2 / 20 °C
6: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C
7: NaBH4 / methanol; CH2Cl2
8: 94 percent / 4-dimethylaminopyridine / CH2Cl2 / 0 °C
9: 83 percent / 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine / benzene / Heating
10: n-Bu4NF / tetrahydrofuran
11: Dess-Martin / CH2Cl2
With
1H-imidazole; 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine; dmap; sodium tetrahydroborate; oxalyl dichloride; Vanadium (III) chloride-(tris-tetrahydrofuran); tetrabutyl ammonium fluoride; hydrogen; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; zinc;
Lindlar's catalyst;
In
tetrahydrofuran; quinoline; methanol; dichloromethane; benzene;
1: Etherification / 2: Reduction / 3: Catalytic hydrogenation / 4: Oxidation / 5: Dimerization / 6: Oxidation / 7: Reduction / 8: thiocarbonylation / 9: reductive dehydroxylation / 10: desilylation / 11: Oxidation;
DOI:10.1016/S0040-4039(99)02062-6
- Guidance literature:
-
Multi-step reaction with 12 steps
1: Pd(PPh3)4; CuI / triethylamine / 20 °C
2: imidazole / CH2Cl2
3: 93 percent / NaBH4 / methanol; CH2Cl2
4: 99 percent / hydrogen / Lindlar / benzene; quinoline
5: 98 percent / Dess-Martin / CH2Cl2
6: 92 percent / VCl3(THF)3; Zn / CH2Cl2 / 20 °C
7: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C
8: NaBH4 / methanol; CH2Cl2
9: 94 percent / 4-dimethylaminopyridine / CH2Cl2 / 0 °C
10: 83 percent / 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine / benzene / Heating
11: n-Bu4NF / tetrahydrofuran
12: Dess-Martin / CH2Cl2
With
1H-imidazole; 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine; dmap; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); oxalyl dichloride; Vanadium (III) chloride-(tris-tetrahydrofuran); tetrabutyl ammonium fluoride; hydrogen; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; zinc;
Lindlar's catalyst;
In
tetrahydrofuran; quinoline; methanol; dichloromethane; triethylamine; benzene;
1: Arylation / 2: Etherification / 3: Reduction / 4: Catalytic hydrogenation / 5: Oxidation / 6: Dimerization / 7: Oxidation / 8: Reduction / 9: thiocarbonylation / 10: reductive dehydroxylation / 11: desilylation / 12: Oxidation;
DOI:10.1016/S0040-4039(99)02062-6
