C₁₂H₁₁Cl₂NO

Base Information

Chemical Name:C₁₂H₁₁Cl₂NO
CAS No.:1515874-61-9
Molecular Formula:C₁₂H₁₁Cl₂NO
Molecular Weight:256.131
Hs Code.:

C<sub>12</sub>H<sub>11</sub>Cl<sub>2</sub>NO

Synonyms:

Suppliers and Price of C₁₂H₁₁Cl₂NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₁Cl₂NO

Chemical Property:

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Technology Process of C₁₂H₁₁Cl₂NO

There total 1 articles about C₁₂H₁₁Cl₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3218-45-9
2,3-dichlorophenylacetonitrile

: 1515874-61-9
C₁₂H₁₁Cl₂NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 66 h / 10 - 30 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 5 - 20 °C

2.2: 5 h / 65 °C

With sodium methylate; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/op4001753

Reference yield:

: 1515874-61-9
C₁₂H₁₁Cl₂NO

: 442628-44-6
2-(2,3-dichlorophenyl)-3-ethoxy-4-fluoro-2-butenenitrile

Guidance literature:: C₁₂H₁₁Cl₂NO; With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -25 - -15 ℃; for 2h;

With N-fluorobis(benzenesulfon)imide; In tetrahydrofuran; toluene; at 0 ℃; for 1h;
DOI:10.1021/op4001753

Reference yield:

: 1515874-61-9
C₁₂H₁₁Cl₂NO

: R(-)-2,4-diamino-5-(2,3-dichlorophenyl)-6-fluoromethylpyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 2 h / -25 - -15 °C

1.2: 1 h / 0 °C

2.1: sodium methylate / methanol / 4.67 h / 25 - 30 °C

3.1: industrial methylated spirits / ethanol; water; dimethyl sulfoxide / 16 h / 65 °C

4.1: triethylamine / water; dimethyl sulfoxide / 0.25 h / 80 °C

4.2: 0.5 h

With sodium methylate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide; toluene;
DOI:10.1021/op4001753