5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole

Base Information

Chemical Name:5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole
CAS No.:132142-84-8
Molecular Formula:C₂₃H₂₇NO₂S
Molecular Weight:381.539
Hs Code.:

5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopen<g>indole

Synonyms:

Suppliers and Price of 5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole

There total 2 articles about 5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R,3R)-2-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-1-{1-[(E)-cyclohexyliminomethyl]-pentyl}-3,5-dimethyl-cyclopentanol

: 132142-84-8,132142-92-8
5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole

Guidance literature:: With sulfuric acid; In isopropyl alcohol; for 1.5h; Yield given; Heating;
DOI:10.1016/S0040-4020(01)86755-7

Reference yield:

: 132142-68-8,132202-08-5,132202-13-2,132202-14-3
3,5-dimethyl-2-(1-phenylsulfonyl-2-pyrrolyl)cyclopentanone

: 132142-84-8,132142-92-8
5-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopenindole

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / 1) THF, a) -20 deg C, 45 min, b) 0 deg C, 15 min, 2) toluene, -77 to -62 deg C, 1h

2: 6percent H₂SO₄ / propan-2-ol / 1.5 h / Heating

With sulfuric acid; lithium diisopropyl amide; In isopropyl alcohol;
DOI:10.1016/S0040-4020(01)86755-7