Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

Base Information

Chemical Name:Ethyl 7-oxospiro[3.5]nonane-6-carboxylate
CAS No.:1424995-17-4
Molecular Formula:C₁₂H₁₈O₃
Molecular Weight:210.273
Hs Code.:

Synonyms:

Suppliers and Price of Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ethyl7-Oxospiro[3.5]nonane-6-carboxylate
100mg
$ 310.00

TRC
Ethyl7-Oxospiro[3.5]nonane-6-carboxylate
10mg
$ 45.00

Chemenu
Ethyl7-oxospiro[3.5]nonane-6-carboxylate 95%
1g
$ 577.00

Alichem
Ethyl7-oxospiro[3.5]nonane-6-carboxylate
1g
$ 708.50

Total 2 raw suppliers

Chemical Property of Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Ethyl7-Oxospiro[3.5]nonane-6-carboxylate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

There total 5 articles about Ethyl 7-oxospiro[3.5]nonane-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869769-27-7
3-[1-(ethoxycarbonylethyl)cyclobutyl]propionic acid ethyl ester

: 1424995-17-4
Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 4h; Heating / reflux;

Reference yield:

: 3779-29-1
diethyl cyclobutane-1,1-dicarboxylate

: 1424995-17-4
Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithiumaluminum hydride bis(tetrahydrofuran) / tetrahydrofuran; toluene / 2.75 h / -20 - 0 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -80 °C

2.2: 5 h / -80 - 10 °C

3.1: lithium chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C

4.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h

5.1: potassium tert-butylate / tetrahydrofuran / 1 h / Reflux

With oxalyl dichloride; lithiumaluminum hydride bis(tetrahydrofuran); palladium 10% on activated carbon; potassium tert-butylate; hydrogen; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 4415-73-0
[1-(hydroxymethyl)cyclobutyl]methanol

: 1424995-17-4
Ethyl 7-oxospiro[3.5]nonane-6-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -80 °C

1.2: 5 h / -80 - 10 °C

2.1: lithium chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h

4.1: potassium tert-butylate / tetrahydrofuran / 1 h / Reflux

With oxalyl dichloride; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;